HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ethanol hydrochloride → HCID 70112645, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ethanol hydrochloride | HCID 21887872 | — |
| Reactant | HCID 70109971 | HCID 70109971 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 70112645 | HCID 70112645 | — |
Reaction Steps
In ethanol was dissolved (3aR*,10aS*)-9-Benzyl-4-methyl-1,2,3,3a,4,9,10,10a-octahydrobenzo[b]-cyclopenta[e][1,4]diazepine produced in Working Example 43. To the solution was added a 2.43N HCl-ethanol solution, which was concentrated under reduced pressure. The concentrate was dissolved in ethanol-ether, which was concentrated to dryness. Amorphous.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05834463 |
| Source dataset | uspto-grants-1998_11 |
| ORD ID | ord-48580f968bb14b80b1aeac083c1ec9a5 |
| Source note | uspto-grants-1998_11 |