HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrochloric Acid → HCID 70111966, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrochloric Acid | HCID 313 | — |
| Reactant | (3aR*,10aS*)-4-(phthalimidoacetyl)-9-(3-pyridylmethyl)-2,3,3a,4,9,10a-hexahydrobenzo[b]cyclopenta[e][1,4]diazepin-10(1H)-one | HCID 70110022 | — |
| Solvent | Diethyl ether ethanol | HCID 21585056 | — |
| Product | HCID 70111966 | HCID 70111966 | — |
Reaction Steps
The (3aR*,10aS*)-4-(phthalimidoacetyl)-9-(3-pyridylmethyl)-2,3,3a,4,9,10a-hexahydrobenzo[b]cyclopenta[e][1,4]diazepin-10(1H)-one, which was obtained in Working Example 116, was made into the corresponding hydrochloride in substantially the same manner as in Working Example 118. m.p. 192°-197° C. (ethanol-diethylether).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05834463 |
| Source dataset | uspto-grants-1998_11 |
| ORD ID | ord-6bc661b405d24d6392ea375d1feaaf55 |
| Source note | uspto-grants-1998_11 |