HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 18940595, compound → HCID 70109608, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 18940595 | HCID 18940595 | — |
| Solvent | Ethyl acetate hexane | HCID 21226206 | — |
| Product | HCID 70109608 | HCID 70109608 | 53% |
Reaction Steps
Using 9-benzyl-7-chloro-2,3,9,10a-tetrahydrobenzo[b]cyclopenta[e][1,4]diazepin-10(1H)-one, the titled compound was synthesized in substantially the same manner as in Working Example 26 in a yield of 53%, m.p. 160°-163° C. (ethylacetate-hexane).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05834463 |
| Source dataset | uspto-grants-1998_11 |
| ORD ID | ord-1b3eb8c38dc64fbfb14f1ec6e09432fb |
| Source note | uspto-grants-1998_11 |