HuagongsheHuagongshe Chemistry Print Report · For research reference only
Diethyl Ether → HCID 70113406, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Diethyl Ether | HCID 3283 | — |
| Reactant | HCID 70112413 | HCID 70112413 | — |
| Product | HCID 70113406 | HCID 70113406 | 76% |
Reaction Steps
Using (3aR*,10aS*)-9-benzyl-4-((3-phenylpropionamido)acetyl)-2,3,3a,4,9,10a-hexahydrobenzo[b]cyclopenta[e][1,4]diazepin-10(1H)-one, the titled compound was synthesized in substantially the same manner as in Working Example 109 in a yield of 76%, m.p. 138°-140° C. (diethyl ether).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05834463 |
| Source dataset | uspto-grants-1998_11 |
| ORD ID | ord-fc8c315a3bc34053815668ba6c3199c3 |
| Source note | uspto-grants-1998_11 |