HuagongsheHuagongshe Chemistry Print Report · For research reference only
Bromoacetyl bromide → HCID 70113834, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Bromoacetyl bromide | HCID 61147 | — |
| Reactant | HCID 70109608 | HCID 70109608 | — |
| Solvent | Ethyl acetate hexane | HCID 21226206 | — |
| Product | HCID 70113834 | HCID 70113834 | 50% |
Reaction Steps
Using (3aR*,10aS*)-9-benzyl-7-chloro-2,3,3a,4,9,10a-hexahydrobenzo[b]cyclopenta[e][1,4]-diazepin-10(1H)-one and bromoacetyl bromide, the titled compound was synthesized in substantially the same manner as in Working Example 122 in a yield of 50%, m.p. 163°-164° C. (ethyl acetate-hexane).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05834463 |
| Source dataset | uspto-grants-1998_11 |
| ORD ID | ord-013366a5e2ea448a86ddca5508546ba1 |
| Source note | uspto-grants-1998_11 |