HuagongsheHuagongshe Chemistry Print Report · For research reference only
Bromoacetyl bromide → HCID 70113643, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Bromoacetyl bromide | HCID 61147 | — |
| Reactant | HCID 70112233 | HCID 70112233 | — |
| Solvent | Ethyl acetate hexane | HCID 21226206 | — |
| Product | HCID 70113643 | HCID 70113643 | 62% |
Reaction Steps
Using (3aR*,10aS*)-9-(2-fluorobenzyl)-2,3,3a,4,9,10a-hexahydrobenzo[b]cyclopenta[e][1,4]-diazepin-10(1H)-one and bromoacetyl bromide, the titled compound was synthesized in substantially the same manner as in Working Example 122 in a yield of 62%, m.p. 198.5°-199.6° C. (ethyl acetate-hexane).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05834463 |
| Source dataset | uspto-grants-1998_11 |
| ORD ID | ord-5a6c62ad6e384b6ca7a944270f238528 |
| Source note | uspto-grants-1998_11 |