HuagongsheHuagongshe Chemistry Print Report · For research reference only
4-Pyridinecarboxaldehyde → HCID 18940621, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 4-Pyridinecarboxaldehyde | HCID 13389 | — |
| Reactant | HCID 18940576 | HCID 18940576 | — |
| Solvent | Diethyl Ether | HCID 3283 | — |
| Product | HCID 18940621 | HCID 18940621 | 36% |
Reaction Steps
Using 1-benzyl-4-methyl-1,3-dihydro-1,5-benzodiazepin-2(2H)-one and isonicotinaldehyde, the titled compound was synthesized in substantially the same manner as in Working Example 144 in a yield of 36%, m.p. 208°-210° C. (diethyl ether).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05834463 |
| Source dataset | uspto-grants-1998_11 |
| ORD ID | ord-0902b722e6874292b5d24d743e86e31c |
| Source note | uspto-grants-1998_11 |