HuagongsheHuagongshe Chemistry Print Report · For research reference only
Bromoacetyl bromide → HCID 70111628, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Bromoacetyl bromide | HCID 61147 | — |
| Reactant | HCID 70112258 | HCID 70112258 | — |
| Product | HCID 70111628 | HCID 70111628 | 72% |
Reaction Steps
Employing (3aR*,10aS*)-9-(2-phenylethyl)-2,3,3a,4,9,10a-hexahydrobenzo[b]cyclopenta-[e][1,4]diazepin-10(1H)-one and bromoacetyl bromide, the titled compound was synthesized by substantially the same procedure as in Working Example 185. Yield 72%. Oily product.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05834463 |
| Source dataset | uspto-grants-1998_11 |
| ORD ID | ord-a7b1e858a84a4b44ab593e0f130f3029 |
| Source note | uspto-grants-1998_11 |