Oxetane → HCID 131720936, compound

HRID 356221Notes

Reaction equation

HRID 356221 reaction equation
[O:1]1[CH2:4][CH2:3][CH2:2]1.[C:5]1(=[O:11])[O:10][CH2:9][CH2:8][CH2:7][CH2:6]1.C([Al](CC)CC)C.O>>[C:5]1(=[O:11])[O:10][CH2:9][CH2:8][CH2:7][CH2:6]1.[O:1]1[CH2:4][CH2:3][CH2:2]1

Participants

4

Reactant 3

HCID 10423OxetaneHCID 10953Delta-ValerolactoneHCID 19429818Triethylalumane--water (1/1)

Product 1

HCID 131720936HCID 131720936, compound

Procedure

According to the ratio for charging as described in Table 2, oxetane and delta-valerolactone (referred to as VL in Table and Figure) were mixed, and polymerized in a bulk state at 60° C. for 24 hours using 0.2% by mol of a triethylaluminum-water (1/0.75) based complex as an initiator based on the total amount of the monomers.

Workup

  1. additionwere mixed
  2. custompolymerized in a bulk state at 60° C. for 24 hours

Sources & evidence

ORD record
ord-5eb6cc29799f4320bb7fc3e47e0a4563
Source dataset
uspto-grants-1998_11
Patent number
US05834567

Reaction notes

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