HuagongsheHuagongshe Chemistry Print Report · For research reference only
3-Methyl-2-butanone → 1-(4-Benzyloxyphenyl)-4-methyl-pent-1-en-3-one
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 3-Methyl-2-butanone | HCID 11251 | — |
| Reactant | Benzaldehyde, 4-(phenylmethoxy)- | HCID 78109 | — |
| Reactant | Barium hydroxide | HCID 6093286 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | 1-(4-Benzyloxyphenyl)-4-methyl-pent-1-en-3-one | HCID 471476 | — |
Reaction Steps
The title compound was prepared as described in the General Method 2 using 81.1 g (942 mmol) of 3-methyl-butan-2-one, 100 g (474 mmol) of 4-benzyloxy benzaldehyde, 10 g of anhydrous barium hydroxide and 500 mL of EtOH.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05834506 |
| Source dataset | uspto-grants-1998_11 |
| ORD ID | ord-5e5820244c6543a186f4751729a479ae |
| Source note | uspto-grants-1998_11 |