HuagongsheHuagongshe Chemistry Print Report · For research reference only
Acetone → HCID 54567841, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Acetone | HCID 180 | — |
| Reactant | 3-Benzyloxybenzaldehyde | HCID 74342 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 54567841 | HCID 54567841 | — |
Reaction Steps
The title compound was prepared as described in General Method 2 using 5.03 g (23.7 mmol) of 3-benzyloxy-benzaldehyde, 150 mL of EtOH, 0.65 mL (11.2 mmol) of acetone, and 0.31 g of Ba(OH)2.(H2O)8. The mixture was heated at room temperature overnight and filtered to give the title compound. 1H NMR (CDCl3) δ 5.08 (s, 4 H), 7.03-7.07 (m, 4 H), 7.22-7.47 (m, 16 H), 7.69 (d, 2 H).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05834506 |
| Source dataset | uspto-grants-1998_11 |
| ORD ID | ord-782d60ad8d7e44daa6114cf9ca12bffd |
| Source note | uspto-grants-1998_11 |