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HRID356573

反应详情

EQUATION

反应方程式

HRID 356573 的结构方程式

REACTANTS

反应物

3
结构：O=Cc1ccccc1
HCID240

Benzaldehyde

C7H6O

结构：CC(C)(C)OC(=O)N[C@@H](Cc1c[nH]c2ccccc12)C(=O)NN
HCID7109657

未命名化合物

结构：[H][H]
HCID178418361

未命名化合物

PRODUCTS

生成物

1
结构：CC(C)(C)OC(=O)N[C@@H](Cc1c[nH]c2ccccc12)C(=O)NNCc1ccccc1
HCID131720940

未命名化合物

AUXILIARIES

试剂、催化剂与溶剂

2
结构：[C].[Pd]
催化剂HCID178418390

未命名化合物

结构：CO
溶剂HCID887

Methanol

CH4O

PROCEDURE

实验过程

In 600 ml of MeOH were dissolved 60.00 g of Boc-Trp-NHNH2 and 21.00 g of benzaldehyde, and the mixture was stirred in the presence of 3.80 g of 10% palladium carbon for 18 hours in a hydrogen stream. Subsequent procedures were carried out in the same manner as in Reference example 21 to obtain the title compound.