Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
1-Methyl-4-iodo-1H-pyrazole → 5,11-Dihydro-11-ethyl-5-methyl-2-(1-methylpyrazol-4-yl)-6H-dipyrido[3,2-b:2',3'-e][1,4]diazepin-6-one
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | 1-Methyl-4-iodo-1H-pyrazole | HCID 2734773 | — |
| 반응물 | 5,11-Dihydro-11-ethyl-5-methyl-2-trifluoromethanesulfonyloxy-6H-dipyrido[3,2-b:2',3'-e][1,4]diazepin-6-one | HCID 10716083 | — |
| 생성물 | 5,11-Dihydro-11-ethyl-5-methyl-2-(1-methylpyrazol-4-yl)-6H-dipyrido[3,2-b:2',3'-e][1,4]diazepin-6-one | HCID 15956279 | — |
반응 단계
The title compound (mp 65°-67° C.) was prepared from 5,11-dihydro-11-ethyl-5-methyl-2-trifluoromethanesulfonyloxy-6H-dipyrido[3,2-b:2',3'-e][1,4]diazepin-6-one and N-methyl-4-iodopyrazole in a manner analogous to that described in Example 1.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US05837704 |
| 출처 데이터셋 | uspto-grants-1998_11 |
| ORD ID | ord-df396e1ee6cb452189b002f2934a5880 |
| 출처 메모 | uspto-grants-1998_11 |