Pyrazole → HCID 15956281, compound

HRID 356598Notes

Reaction equation

HRID 356598 reaction equation
[CH3:1][N:2]1[C:8](=[O:9])[C:7]2[CH:10]=[CH:11][CH:12]=[N:13][C:6]=2[N:5]([CH2:14][CH2:15][CH3:16])[C:4]2[N:17]=[C:18](OS(C(F)(F)F)(=O)=O)[CH:19]=[CH:20][C:3]1=2.[NH:29]1[CH:33]=[CH:32][CH:31]=[N:30]1>>[CH3:1][N:2]1[C:8](=[O:9])[C:7]2[CH:10]=[CH:11][CH:12]=[N:13][C:6]=2[N:5]([CH2:14][CH2:15][CH3:16])[C:4]2[N:17]=[C:18]([C:32]3[CH:33]=[N:29][NH:30][CH:31]=3)[CH:19]=[CH:20][C:3]1=2

Participants

3

Reactant 2

HCID 1048PyrazoleHCID 18938882HCID 18938882, compound

Product 1

HCID 15956281HCID 15956281, compound

Procedure

The title compound (mp 206°-207° C.) was prepared from 5,11-dihydro-5-methyl-11-n-propyl-2-trifluoromethanesulfonyloxy-6H-dipyrido[3,2-b:2',3'-e][1,4]diazepin-6-one and 4-stannyl)pyrazole in a manner analogous to that described in Example 1.

Sources & evidence

ORD record
ord-b094be09ef4248189316148d5588545e
Source dataset
uspto-grants-1998_11
Patent number
US05837704

Reaction notes

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