HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ethyl Bromide → HCID 178477469, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ethyl Bromide | HCID 6332 | — |
| Reactant | Ethyl Acetate | HCID 8857 | — |
| Reactant | HCID 178514160 | HCID 178514160 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 178477469 | HCID 178477469 | — |
Reaction Steps
4 gram N-phenylisothiourea (33 mmol) and 5 ml ethyl bromide were refluxed for 10 hours in ethanol. Again 5 ml ethyl bromide was added. The reaction course was followed by thin layer chromatography (ethylacetate/petroleumether 3:7). Subsequently the solvent was evaporated and the residue crystallised from ethanol/ethylacetate.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05837718 |
| Source dataset | uspto-grants-1998_11 |
| ORD ID | ord-9f8b5cebd00640a1859fa440c4f3e2d6 |
| Source note | uspto-grants-1998_11 |