HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 86753335, compound → HCID 86753334, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 86753335 | HCID 86753335 | — |
| Solvent | Ethylene Glycol | HCID 174 | — |
| Product | HCID 86753334 | HCID 86753334 | — |
Reaction Steps
In analogy to Example 45, by reacting 5-isopropyl-pyridine-2-sulphonic acid [6-chloro-2-(3-methoxy-benzyl)-5-(2-methoxy- phenoxy)-pyrimidin-4-yl]-amide with Na in ethylene glycol there was obtained 5-isopropyl-pyridine-2-sulphonic acid [6-(2-hydroxy-ethoxy)-2-(3-methoxy-benzyl)-5-(2-methoxy-phenoxy)-pyrimidin-4-yl]-amide as a white foam. MS: 579.3 (M-H)
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05837708 |
| Source dataset | uspto-grants-1998_11 |
| ORD ID | ord-58d5f4c0cae04fb682b36f225116b8bf |
| Source note | uspto-grants-1998_11 |