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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 356997Generated: October 28, 2026

Phosphoric Acid → HCID 67615143, compound

https://huagongshe.com/reaction/356997

Reaction equation

Participants

RoleNameHCIDCharge
ReactantPhosphoric AcidHCID 1004—
ReactantPhosphorus oxide (P4O10)HCID 14812—
ReactantHCID 54130696HCID 54130696—
ProductHCID 67615143HCID 6761514350%

Reaction Conditions

Temperature60 °C

Reaction Steps

A mixture of 5-hydroxy-3-(quinol-4-ylmethylene)-2-oxindole (2.883 g, 10 mmol) and phosphoric acid 85% (13 g) and phosphorous pentoxide (10 g) was heated for 2 h at 60° C. The usual work-up gave the title compound in about 50% yield.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS05840745
Source datasetuspto-grants-1998_11
ORD IDord-025fad3f915d4228874720089fd13d9a
Source noteuspto-grants-1998_11