Hydrochloric Acid → HCID 131720952, compound

HRID 356999Notes

Reaction equation

HRID 356999 reaction equation
[NH2:1][CH2:2][C:3]1[CH:4]=[C:5]2[C:9](=[CH:10][CH:11]=1)[NH:8][C:7](=[O:12])[C:6]2=[CH:13][C:14]1[C:23]2[C:18](=[CH:19][CH:20]=[CH:21][CH:22]=2)[N:17]=[CH:16][CH:15]=1.[ClH:24]>C(O)C>[ClH:24].[NH2:1][CH2:2][C:3]1[CH:4]=[C:5]2[C:9](=[CH:10][CH:11]=1)[NH:8][C:7](=[O:12])[C:6]2=[CH:13][C:14]1[C:23]2[C:18](=[CH:19][CH:20]=[CH:21][CH:22]=2)[N:17]=[CH:16][CH:15]=1

Participants

4

Reactant 2

HCID 313Hydrochloric AcidHCID 67615454HCID 67615454, compound

Product 1

HCID 131720952HCID 131720952, compoundYield 100%

Reagents, catalysts & solvents 1

HCID 702EthanolSolvent

Procedure

To a solution of 5-aminomethyl-3-(quinol-4-ylmethylene)-2-oxindole (3.014 g, 10 mmol) in ethanol (10 ml) was added 1N hydrochloric acid (2 ml, 2 mmol) and the resulting mixture was evaporated to dryness under vacuum, thus giving pure title compound in about 100% yield.

Workup

  1. customthe resulting mixture was evaporated to dryness under vacuum

Sources & evidence

ORD record
ord-5771d1007d4342018bd1390bf164f58a
Source dataset
uspto-grants-1998_11
Patent number
US05840745

Reaction notes

Loading…