HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrochloric Acid → HCID 73472963, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrochloric Acid | HCID 313 | — |
| Reactant | HCID 57004843 | HCID 57004843 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | HCID 73472963 | HCID 73472963 | — |
Reaction Steps
To a solution of 1.56 g (3.45 mmol) of 5-(4-phenyl-butylidene)-3-[4-(imidazo[1,2-a]pyridin-5-ylthio)butyl]thiazolidine-2,4-dione in 50 ml of methanol, 0.4 ml of concentrated hydrochloric acid was added. After the solvent was distilled off, the residue was washed with diethyl ether to yield 1.47 g (87%, light yellow foamy substance) of the desired product.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05840732 |
| Source dataset | uspto-grants-1998_11 |
| ORD ID | ord-68ea1383f5e046b482049d2ad50eba15 |
| Source note | uspto-grants-1998_11 |