Hydrogen chloride-ethyl acetate → HCID 73472935, compound

Participants

Reaction Steps

To a methanol solution of 1.052 g (2.79 mmol) of 5-butylidene-3-[4-(imidazo[1,2-c]pyrimidin-5-ylthio)butyl]thiazolidine-2,4-dione, 3 ml of 4N hydrochloric acid-ethyl acetate was added, followed by stirring, after which the solvent was distilled off, to yield 0.914 g (79.3%, white powder) of the desired product.

Provenance & Evidence