HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrochloric Acid → HCID 73472900, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrochloric Acid | HCID 313 | — |
| Reactant | HCID 57245948 | HCID 57245948 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | HCID 73472900 | HCID 73472900 | — |
Reaction Steps
To a solution of 250 mg (0.55 mmol) of 5-butylidene-3-[4-(3-trifluoroacetylimidazo[1,2-a]pyridin-8-yloxy)butyl]-thiazolidine-2,4-dione in 5 ml of methanol, 0.05 ml of concentrated hydrochloric acid was added. After the solvent was distilled off, the residue was washed with diethyl ether to yield 290 mg (100%, white solid) of the desired product.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05840732 |
| Source dataset | uspto-grants-1998_11 |
| ORD ID | ord-f88b08e21e0a421ca83da02795de3e3a |
| Source note | uspto-grants-1998_11 |