HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrochloric Acid → HCID 86753349, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrochloric Acid | HCID 313 | — |
| Reactant | 5-Carboethoxymethylene-3-[4-(imidazo[1,2-a]pyridin-5-ylthio)butyl]thiazolidine-2,4-dione | HCID 54565604 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | HCID 86753349 | HCID 86753349 | — |
Reaction Steps
To a solution of 0.70 g (1.73 mmol) of 5-carboethoxymethylene-3-[4-(imidazo[1,2-a]pyridin-5-ylthio)butyl]thiazolidine-2,4-dione in 20 ml of methanol, 0.20 ml of concentrated hydrochloric acid was added, followed by stirring, after which the solvent was distilled off. The residue was washed with diethyl ether to yield 0.74 g (96.8%, white solid) of the desired product.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05840732 |
| Source dataset | uspto-grants-1998_11 |
| ORD ID | ord-2369fe53fef34bbeb5d1fcb2db1d9feb |
| Source note | uspto-grants-1998_11 |