HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrochloric Acid → HCID 73472979, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrochloric Acid | HCID 313 | — |
| Reactant | HCID 57190382 | HCID 57190382 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | HCID 73472979 | HCID 73472979 | — |
Reaction Steps
To a solution of 310 mg (0.74 mmol) of 5-butylidene-3-[5-(imidazo[1,2-a]pyridin-5-ylthio)-3,3-dimethylpentyl]thiazolidine-2,4-dione in 5 ml methanol, 0.01 ml of concentrated hydrochloric acid was added. After the solvent was distilled off, the residue was washed with diethyl ether to yield 320 mg (95.0%, light yellow solid) of the desired product.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05840732 |
| Source dataset | uspto-grants-1998_11 |
| ORD ID | ord-3e76545827b3499ea20f83740bb698d9 |
| Source note | uspto-grants-1998_11 |