HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrochloric Acid → HCID 73472904, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrochloric Acid | HCID 313 | — |
| Reactant | HCID 57320792 | HCID 57320792 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | HCID 73472904 | HCID 73472904 | — |
Reaction Steps
To a solution of 1.70 g (4.36 mmol) of 5-pentylidene-3-[4-(imidazo[1,2-a]pyridin-5-ylthio)butyl]thiazolidine-2,4-dione in 30 ml of methanol, 0.42 ml of concentrated hydrochloric acid was added. After the solvent was distilled off, the residue was washed with diethyl ether to yield 1.77 g (95.3%, yellow-orange oily substance) of the desired product.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05840732 |
| Source dataset | uspto-grants-1998_11 |
| ORD ID | ord-c147796933a849d194791c174ecae39f |
| Source note | uspto-grants-1998_11 |