HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrogen chloride-ethyl acetate → HCID 70205491, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrogen chloride-ethyl acetate | HCID 21866389 | — |
| Reactant | HCID 53634368 | HCID 53634368 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | HCID 70205491 | HCID 70205491 | — |
Reaction Steps
To a methanol solution of 75 mg (0.15 mmol) of imidazo[1,2-a]pyridin-5-acetic [3-(1,1,6,8-tetraoxo-9-phenyl-2,3,4,8-tetrahydropyrimido[6,1-b][1,3]thiazine-7-yl)propyl]amide, 0.1 ml of 4N hydrochloric acid-ethyl acetate was added, followed by stirring, after which the solvent was distilled off, to yield 75 mg (92.0%, light yellow oily substance) of the desired product.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05840732 |
| Source dataset | uspto-grants-1998_11 |
| ORD ID | ord-5e7705222da641f48ddc89624a949fc4 |
| Source note | uspto-grants-1998_11 |