HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 54002888, compound → 2-[{4-(2-Methoxyethoxy)ethoxy-3,5-dimethylpyridine-2-yl}methylthio]-1H-benzimidazole
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 54002888 | HCID 54002888 | — |
| Reactant | HCID 178527775 | HCID 178527775 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | 2-[{4-(2-Methoxyethoxy)ethoxy-3,5-dimethylpyridine-2-yl}methylthio]-1H-benzimidazole | HCID 15166324 | 26.5% |
Reaction Steps
A mixture comprising 3.0 g of {4-(2-methoxyethoxy)ethoxy-3,5-dimethylpyridine-2-yl}methyl methanesulfonate, 1.17 g of 2-mercaptobenzimidazole and 30 ml of ethanol was stirred at a room temperature for one hour and distilled to remove the ethanol. The residue was purified by silica gel column chromatography to obtain 0.8 g of the title compound.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05840910 |
| Source dataset | uspto-grants-1998_11 |
| ORD ID | ord-bbb2b72d7702454e86ce20965938a022 |
| Source note | uspto-grants-1998_11 |