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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 357565Generated: October 29, 2026

HCID 54002888, compound → 2-[{4-(2-Methoxyethoxy)ethoxy-3,5-dimethylpyridine-2-yl}methylthio]-1H-benzimidazole

https://huagongshe.com/reaction/357565

Reaction equation

Participants

RoleNameHCIDCharge
ReactantHCID 54002888HCID 54002888—
ReactantHCID 178527775HCID 178527775—
SolventEthanolHCID 702—
Product2-[{4-(2-Methoxyethoxy)ethoxy-3,5-dimethylpyridine-2-yl}methylthio]-1H-benzimidazoleHCID 1516632426.5%

Reaction Steps

A mixture comprising 3.0 g of {4-(2-methoxyethoxy)ethoxy-3,5-dimethylpyridine-2-yl}methyl methanesulfonate, 1.17 g of 2-mercaptobenzimidazole and 30 ml of ethanol was stirred at a room temperature for one hour and distilled to remove the ethanol. The residue was purified by silica gel column chromatography to obtain 0.8 g of the title compound.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS05840910
Source datasetuspto-grants-1998_11
ORD IDord-bbb2b72d7702454e86ce20965938a022
Source noteuspto-grants-1998_11