HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrochloric Acid → Benzenecarboximidic acid, 3-acetyl-, ethyl ester, hydrochloride
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrochloric Acid | HCID 313 | — |
| Reactant | Ethanol | HCID 702 | — |
| Reactant | 3-Acetylbenzonitrile | HCID 80222 | — |
| Solvent | Diethyl Ether | HCID 3283 | — |
| Product | Benzenecarboximidic acid, 3-acetyl-, ethyl ester, hydrochloride | HCID 12289426 | — |
Reaction Steps
A solution of 7.25 g (0.05 mol) of 3-acetylbenzonitrile (Aldrich, Buchs, Switzerland; Cat. No. 29,221-4) in 150 ml of diethyl ether and 4.5 ml of ethanol is saturated at 0° C. with dry hydrochloric acid gas and then left to stand at 0° C. for 2 days. The product that has crystallized out is filtered off and the title compound is obtained after recrystallization from ethanol/diethyl ether, m.p. 110° C. (decomp.).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05840911 |
| Source dataset | uspto-grants-1998_11 |
| ORD ID | ord-8d361d0a4c154a149f4e969a52691a6b |
| Source note | uspto-grants-1998_11 |