Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | Formic Acid | HCID 284 | — |
| Reactant | 3-Fluorobenzotrichloride | HCID 67866 | — |
| Catalyst | Ferrous Chloride | HCID 24458 | — |
| Product | 3-Fluorobenzoyl chloride | HCID 74376 | — |
Reaction Steps
300 g of 3-fluorobenzotrichloride and 1.5 g of iron chloride are placed in an apparatus comprising a 1 l four necked flask equipped with stirrer, thermometer, reflux condenser and dropping funnel. The mixture was heated to 80° C. A total of 53 ml of formic acid were then added over 5 hours in such a manner that the temperature could readily be maintained.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| Patent number | US05840975 |
|---|
| Source dataset | uspto-grants-1998_11 |
|---|
| ORD ID | ord-33f9cfd201e04a34a6e4ad53643cc773 |
|---|
| Source note | uspto-grants-1998_11 |
|---|
