Back
HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 357724Generated: October 25, 2026

Diisopropyl Ether → (R)-2-bromo-1-(3-chlorophenyl)ethanol

https://huagongshe.com/reaction/357724

Reaction equation

Participants

RoleNameHCIDCharge
ReactantDiisopropyl EtherHCID 7914—
Reactant2-Bromo-1-(3-chlorophenyl)ethanolHCID 9964694—
Product(R)-2-bromo-1-(3-chlorophenyl)ethanolHCID 11075396—

Reaction Steps

Diisopropyl ether was added to a mixture of 100 mg (0.4 mmol) of 2-bromo-1-(3-chlorophenyl)ethanol, 20 mg of TOYOCHIMU LIP (available from Toyobo Co., Ltd.) and 0.3 mmol of each of the various acid anhydrides shown in Table 3 was to make the total volume to 1 ml. These reaction mixtures were respectively allowed to undergo reaction at a temperature of 27° C. for 98 hours. The results are set forth in Table 3.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS05841001
Source datasetuspto-grants-1998_11
ORD IDord-8af97dab936b4dbda8044b95a5688946
Source noteuspto-grants-1998_11