HuagongsheHuagongshe Chemistry Print Report · For research reference only
(3-Bromopropyl)benzene → HCID 86753002, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | (3-Bromopropyl)benzene | HCID 12503 | — |
| Reactant | Benzenesulfonothioic acid, 4-methyl-, potassium salt (1:1) | HCID 23662126 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 86753002 | HCID 86753002 | — |
Reaction Steps
The title compound was prepared as described in General Method 2 using 1-bromo-3-phenylpropane (0.044 mmol), potassium thiotosylate (0.044 mmol) and absolute ethanol (125 mL) to give an oil which was used without purification. 1H NMR (CDCl3) δ 1.95 (quint., 2 H), 2.459 (s, 3 H), 2.63 (t, 2 H), 2.95 (t, 2 H), 7.0-7.4 (m, 8 H), 7.7 (d, 2 H).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05840751 |
| Source dataset | uspto-grants-1998_11 |
| ORD ID | ord-f8d73daa2a704338a9e533a0f3acd15a |
| Source note | uspto-grants-1998_11 |