HuagongsheHuagongshe Chemistry Print Report · For research reference only
Acrolein → HCID 13088566, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Acrolein | HCID 7847 | — |
| Reactant | 5,5-Dimethyl-1,3-hexadiene | HCID 142069 | — |
| Reactant | HCID 13088567 | HCID 13088567 | — |
| Product | HCID 13088566 | HCID 13088566 | 30% |
Reaction Steps
Molar amounts of tert.-butylbutadiene and acrolein are refluxed for 6-8 hours. A mixture of about 70% of 4-tert.-butyl-cyclohex-3-ene-1-carboxaldehyde and about 30% of 3-tert.-butyl-cyclohex-3-ene-1-carboxaldehyde is obtained in a yield of about 80%. Boiling point: 112° C./28 mbar.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04464370 |
| Source dataset | uspto-grants-1984_08 |
| ORD ID | ord-9ca5366014a948e9a3738c128a37ac97 |
| Source note | uspto-grants-1984_08 |