HuagongsheHuagongshe Chemistry Print Report · For research reference only
Aniline → HCID 12806756, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Aniline | HCID 6115 | — |
| Reactant | 4,8-dichloroquinazoline | HCID 247267 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 12806756 | HCID 12806756 | 49.3% |
Reaction Steps
15 ml of ethanol were added to a mixture of 3.0 g of 4,8-dichloroquinazoline and 1.9 g of aniline, and then the mixture was heated. The reagents dissolved and immediately solidified. After cooling, the solidified product was collected, washed with ethanol and then recrystallized from ethanol to give 1.9 g (yield 48%) of the desired Compound No. 13 in the form of colourless crystals having a melting point of 206° C. (with decomposition).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04464375 |
| Source dataset | uspto-grants-1984_08 |
| ORD ID | ord-9b8178506e12470095f437111132c73c |
| Source note | uspto-grants-1984_08 |