N-Methylaniline → HCID 12774510, compound

Participants

Reaction Steps

A solution of 3.0 g of 4,7-dichloroquinazoline and 1.7 g of N-methylaniline in 10 ml of ethanol was heated for 10 minutes. After completion of the reaction, the ethanol was distilled off and the resulting crystals were recrystallized from a small amount of ethanol to give 2.4 g (yield 46%) of the desired Compound No. 56 in the form of pale yellow granules melting at 230°-233° C. (with decomposition).

Provenance & Evidence