Hydrochloric Acid → HCID 20450002, compound

Participants

Reaction Steps

For conversion into the hydrochloride, the base is dissolved in isopropanol and treated with an equivalent amount of hydrogen chloride in isopropanol. After evaporation of the solvent and recrystallization of the hydrochloride from a ten-fold amount of water, there is obtained 1-(aminomethyl)-8-chloro-6-(2-fluorophenyl)-4H-s-triazolo[4,3-a][1]benzazepine hydrochloride of melting point 246°-248° (decomposition).

Provenance & Evidence