HuagongsheHuagongshe Chemistry Print Report · For research reference only
3-Mercaptopropionic Acid → HCID 70508087, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 3-Mercaptopropionic Acid | HCID 6514 | — |
| Reactant | HCID 20449999 | HCID 20449999 | — |
| Solvent | Hydrochloric Acid | HCID 313 | — |
| Product | HCID 70508087 | HCID 70508087 | — |
Reaction Steps
107.3 g of 5-acetamino-2-amino-2'-chlorobenzhydrol are heated to 90° for 1 hour together with 36.8 g of 3-mercaptopropionic acid in 290 ml of 6N hydrochloric acid. After cooling, the crystals are filtered off. There is obtained 3-[(2,5-diaminophenyl)(2-chlorophenyl)methylthio]propionic acid dihydrochloride of melting point 234°-235° (decomposition).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04464300 |
| Source dataset | uspto-grants-1984_08 |
| ORD ID | ord-38f309781e714ac19cdbd5258f539c6b |
| Source note | uspto-grants-1984_08 |