HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ethyl isocyanate → HCID 13337913, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ethyl isocyanate | HCID 8022 | — |
| Reactant | N-Phenylglycine | HCID 66025 | — |
| Solvent | Toluene | HCID 1140 | — |
| Product | HCID 13337913 | HCID 13337913 | 42% |
Reaction Steps
A mixture of N-phenyl glycine (30.2 grams, 0.2 moles), ethylisocyanate (17.8 grams, 0.25 moles) and 30 ml of toluene was refluxed for 9 hours and allowed to stand overnight at room temperature (21° C.). The suspended product was collected by filtration and washed with toluene. After drying (21° C.) it was crystallized from ethanol to produce 17 grams (42% yield) of the above-identified product having a melting point of about 142° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04464387 |
| Source dataset | uspto-grants-1984_08 |
| ORD ID | ord-aa519dd2f91746e8b99db034310ea6cb |
| Source note | uspto-grants-1984_08 |