HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydroxyamine hydrochloride → HCID 86739589, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydroxyamine hydrochloride | HCID 443297 | — |
| Reactant | HCID 70509511 | HCID 70509511 | — |
| Product | HCID 86739589 | HCID 86739589 | — |
Reaction Steps
32.2 g of 2-(3-BOC-methylaminophenyl)-glyoxylic acid are reacted with 13.8 g of hydroxylamine hydrochloride in the manner described in Example 4. Crystallisation from CH2Cl2 /CH3OH/ether/hexane yields 2-(3-BOC-methylaminophenyl)-2-hydroxyiminoacetic acid. M.p. 135° (decomposition). IR: 3620, 3600-2300 (wide), 1688, 1600, 1590 (shoulder) cm-1 (CH2Cl2).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04464366 |
| Source dataset | uspto-grants-1984_08 |
| ORD ID | ord-d3069b006f5c4617b762822454a9478d |
| Source note | uspto-grants-1984_08 |