Hydroxyamine hydrochloride → HCID 86739590, compound

HRID 358172Notes

Reaction equation

HRID 358172 reaction equation
[C:1]([C:8]1[C:9]([NH2:19])=[C:10]([C:14](=O)[C:15]([OH:17])=[O:16])[CH:11]=[CH:12][CH:13]=1)([O:3][C:4]([CH3:7])([CH3:6])[CH3:5])=[O:2].Cl.[NH2:21][OH:22]>>[C:1]([C:8]1[C:9]([NH2:19])=[C:10]([C:14](=[N:21][OH:22])[C:15]([OH:17])=[O:16])[CH:11]=[CH:12][CH:13]=1)([O:3][C:4]([CH3:7])([CH3:6])[CH3:5])=[O:2]

Participants

3

Reactant 2

HCID 443297Hydroxyamine hydrochlorideHCID 70508114HCID 70508114, compound

Product 1

HCID 86739590HCID 86739590, compound

Procedure

11.7 g of 2-(3-BOC-aminophenyl)-glyoxylic acid are reacted with 5 g of hydroxylamine hydrochloride in the manner described in Example 4. 2-(3-BOC-Aminophenyl)-2-hydroxyiminoacetic acid is obtained.

Sources & evidence

ORD record
ord-80e381ae546444bf98ecc2faa666eef8
Source dataset
uspto-grants-1984_08
Patent number
US04464366

Reaction notes

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