HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methyl[1-(2-methylphenyl)ethyl]amine → HCID 15589250, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methyl[1-(2-methylphenyl)ethyl]amine | HCID 16771015 | — |
| Reactant | HCID 20449307 | HCID 20449307 | — |
| Product | HCID 15589250 | HCID 15589250 | 93.6% |
Reaction Steps
A mixture consisting of 9.5 g of α,α-diethylbenzylisocyanate and 7.5 g of N-(2-methyl-α-methylbenzyl)-N-methylamine was allowed to stand for 3 hours at room temperature. The white deposit formed was then filtered off. Washing with n-hexane and recrystallization from ethanol gave 15.9 g of the product, mp 93.0°-94.0° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04465509 |
| Source dataset | uspto-grants-1984_08 |
| ORD ID | ord-4f534a0195fa4771a28d11d2e4b84d17 |
| Source note | uspto-grants-1984_08 |