HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methyl isothiocyanate → HCID 178486106, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methyl isothiocyanate | HCID 11167 | — |
| Reactant | 1-(4-Chlorophenyl)-4,5-dihydro-1H-pyrazol-3-amine | HCID 12551450 | — |
| Product | HCID 178486106 | HCID 178486106 | — |
Reaction Steps
3-Amino-1-(4-chlorophenyl)-2-pyrazoline (1.5 g) (prepared in Reference Example 6 of our European patent specification No. 22-578) and methylisothiocyanate (1.02 g) were heated together at 100° for two hours. The crude product was ground under methanol, collected by filtration, and recrystallised from acetone to yield 3-(3-methylthioureido)-1-(4-chlorophenyl)-2-pyrazoline, m.p. 237°.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04465685 |
| Source dataset | uspto-grants-1984_08 |
| ORD ID | ord-f7322818cc2c48fba8a956de47e50faf |
| Source note | uspto-grants-1984_08 |