HuagongsheHuagongshe Chemistry Print Report · For research reference only
Isopropanol → Isopropyl Trichloroacrylate
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Isopropanol | HCID 3776 | — |
| Reactant | 2,3,3-Trichloro-2-propenoyl chloride | HCID 13153 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Product | Isopropyl Trichloroacrylate | HCID 13362187 | — |
Reaction Steps
A solution of 6.5 gms (0.108 moles) isopropyl alcohol, 20 gms (0.013 moles) trichloro acryloyl chloride and 100 ml methylene chloride was stirred for 72 hours. The solvent was stripped and the product was used in subsequent reactions without further purification.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04465690 |
| Source dataset | uspto-grants-1984_08 |
| ORD ID | ord-4cc9112742054be59544a64647003c56 |
| Source note | uspto-grants-1984_08 |