Isopropanol → Isopropyl Trichloroacrylate

HRID 358223Notes

Reaction equation

HRID 358223 reaction equation
[CH:1]([OH:4])([CH3:3])[CH3:2].[Cl:5][C:6](=[C:10]([Cl:12])[Cl:11])[C:7](Cl)=[O:8]>C(Cl)Cl>[Cl:11][C:10]([Cl:12])=[C:6]([Cl:5])[C:7]([O:4][CH:1]([CH3:3])[CH3:2])=[O:8]

Participants

4

Reactant 2

HCID 3776IsopropanolHCID 131532,3,3-Trichloro-2-propenoyl chloride

Product 1

HCID 13362187Isopropyl Trichloroacrylate

Reagents, catalysts & solvents 1

HCID 6344DichloromethaneSolvent

Procedure

A solution of 6.5 gms (0.108 moles) isopropyl alcohol, 20 gms (0.013 moles) trichloro acryloyl chloride and 100 ml methylene chloride was stirred for 72 hours. The solvent was stripped and the product was used in subsequent reactions without further purification.

Workup

  1. customthe product was used in subsequent reactions without further purification

Sources & evidence

ORD record
ord-4cc9112742054be59544a64647003c56
Source dataset
uspto-grants-1984_08
Patent number
US04465690

Reaction notes

Loading…