HRID358262

反应详情

EQUATION

反应方程式

HRID 358262 的结构方程式

AUXILIARIES

试剂、催化剂与溶剂

1

PROCEDURE

实验过程

A solution of 2.3 gm of 4-(4-aminophenyl)-1-H-imidazole and 1.15 gm of methyl isothiocyanate in 30 ml of ethanol was refluxed for thirty minutes and evaporated to dryness. The oily base so obtained was purified by conversion into the corresponding hydrochloride salt by bubbling gaseous hydrochloric acid in isopropanol. The desired thiourea was obtained as a white solid.

WORKUP

后处理

  1. customevaporated to dryness
  2. customThe oily base so obtained
  3. customwas purified by conversion into the corresponding hydrochloride salt
  4. customby bubbling gaseous hydrochloric acid in isopropanol