HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methyl isothiocyanate → HCID 178486097, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methyl isothiocyanate | HCID 11167 | — |
| Reactant | HCID 178507418 | HCID 178507418 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 178486097 | HCID 178486097 | — |
Reaction Steps
A solution of 2.3 gm of 4-(4-aminophenyl)-1-H-imidazole and 1.15 gm of methyl isothiocyanate in 30 ml of ethanol was refluxed for thirty minutes and evaporated to dryness. The oily base so obtained was purified by conversion into the corresponding hydrochloride salt by bubbling gaseous hydrochloric acid in isopropanol. The desired thiourea was obtained as a white solid.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04465841 |
| Source dataset | uspto-grants-1984_08 |
| ORD ID | ord-3b6a72acc242468fa129b70ab27e32a6 |
| Source note | uspto-grants-1984_08 |