Iaa-94 → 2-Butyl-6,7-dichloro-2-cyclopentyl-5-hydroxy-1-indanone

Participants

Role	Name	HCID	Charge
Reactant	Iaa-94	HCID 3667	—
Reactant	((2-n-butyl-6,7-dichloro-2-cyclopentyl-2,3-dihydro-1-oxo-1H-inden-5-yl)oxy)acetic acid, (+)-	HCID 5017	—
Product	2-Butyl-6,7-dichloro-2-cyclopentyl-5-hydroxy-1-indanone	HCID 12761136	—

Reaction Steps

By following substantially the procedure in Example 8, Step A, but substituting for (+)[(6,7-dichloro-2-cyclopentyl-2,3-dihydro-2-methyl-1-oxo-1H-inden-5-yl)oxy]acetic acid an equimolar quantity of (+)[(2-butyl-6,7-dichloro-2-cyclopentyl-2,3-dihydro-1-oxo-1H-inden-5-yl)oxy]acetic acid, there is obtained (+)2-butyl-6,7-dichloro-2-cyclopentyl-2,3-dihydro-5-hydroxy-1H-inden-1-one which is used in Step C without further purification.

Provenance & Evidence

DOI	10.6084/m9.figshare.5104873.v1
Patent number	US04465850
Source dataset	uspto-grants-1984_08
ORD ID	ord-ab50f5bdfad94891969c7446d3351bf9
Source note	uspto-grants-1984_08