Phenyl isocyanate → HCID 70514536, compound

HRID 358281Notes

Reaction equation

HRID 358281 reaction equation
[CH2:1]([C:4]1[CH:9]=[CH:8][CH:7]=[CH:6][C:5]=1[OH:10])[CH:2]=[CH2:3].[C:11]1([N:17]=[C:18]=[O:19])[CH:16]=[CH:15][CH:14]=[CH:13][CH:12]=1>N1C=CC=CC=1>[CH2:1]([C:4]1[CH:9]=[CH:8][CH:7]=[CH:6][C:5]=1[OH:10])[CH:2]=[CH2:3].[C:11]1([NH:17][C:18]([O:10][CH2:5][CH3:4])=[O:19])[CH:16]=[CH:15][CH:14]=[CH:13][CH:12]=1

Participants

4

Reactant 2

HCID 7672Phenyl isocyanateHCID 156242-Allylphenol

Product 1

HCID 70514536HCID 70514536, compound

Reagents, catalysts & solvents 1

HCID 1049PyridineSolvent

Procedure

A mixture of 13.5 g. of 2-allyl-phenol, 13.1 g. of phenylisocyanate and 0.5 g. of pyridine is kept at 100° C. for five minutes. Petroleum ether is added whereupon the precipitated crystals are filtered off with suction and washed with petroleum ether to give 2-allyl-phenol-phenylurethane, melting at 108° C. to 109° C.

Workup

  1. additionA mixture of 13.5 g
  2. filtrationare filtered off with suction
  3. washwashed with petroleum ether

Sources & evidence

ORD record
ord-5607d6118bf94a2fb1d5f1f07e9d45c7
Source dataset
uspto-grants-1984_08
Patent number
US04465855

Reaction notes

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