HuagongsheHuagongshe Chemistry Print Report · For research reference only
Phenyl isocyanate → HCID 70514536, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Phenyl isocyanate | HCID 7672 | — |
| Reactant | 2-Allylphenol | HCID 15624 | — |
| Solvent | Pyridine | HCID 1049 | — |
| Product | HCID 70514536 | HCID 70514536 | — |
Reaction Steps
A mixture of 13.5 g. of 2-allyl-phenol, 13.1 g. of phenylisocyanate and 0.5 g. of pyridine is kept at 100° C. for five minutes. Petroleum ether is added whereupon the precipitated crystals are filtered off with suction and washed with petroleum ether to give 2-allyl-phenol-phenylurethane, melting at 108° C. to 109° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04465855 |
| Source dataset | uspto-grants-1984_08 |
| ORD ID | ord-5607d6118bf94a2fb1d5f1f07e9d45c7 |
| Source note | uspto-grants-1984_08 |