HuagongsheHuagongshe Chemistry Print Report · For research reference only
3-Amino-4-methoxycyclobut-3-ene-1,2-dione → HCID 20448693, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 3-Amino-4-methoxycyclobut-3-ene-1,2-dione | HCID 13452205 | — |
| Reactant | HCID 14625101 | HCID 14625101 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 20448693 | HCID 20448693 | 66% |
Reaction Steps
1-Amino-2-methoxy-cyclobut-1-ene-3,4-dione (0.5 g) and 3-[4-(dimethylaminomethyl)pyrid-2-yloxy]prop-1-yl-amine (0.85 g) were refluxed in ethanol in a similar manner to Example 1. The solid obtained was recrystallised from ethanol to give the title product, (0.79 g), m.p. 212°-4° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04466970 |
| Source dataset | uspto-grants-1984_08 |
| ORD ID | ord-13b4d6e8bb72484dba5827d624dd1bbf |
| Source note | uspto-grants-1984_08 |