HuagongsheHuagongshe Chemistry Print Report · For research reference only
Diazomethane → HCID 13448671, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Diazomethane | HCID 9550 | — |
| Reactant | 3-Hexynoic acid | HCID 5312635 | — |
| Catalyst | Acetic Acid | HCID 176 | — |
| Solvent | Diethyl Ether | HCID 3283 | — |
| Product | HCID 13448671 | HCID 13448671 | — |
Reaction Steps
A solution of 5.9 g of 3-hexynoic acid in 50 ml of ether is treated with a slight excess of ethereal diazomethane solution. A few drops of glacial acetic acid are added to the mixture, the mixture is concentrated in vacuo and then distilled. 5.65 g of the title compound are obtained: b.p. 62° C. (5 mm).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04466969 |
| Source dataset | uspto-grants-1984_08 |
| ORD ID | ord-f9726011908648edaaa2665197868482 |
| Source note | uspto-grants-1984_08 |