HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 19912998, compound → HCID 19912992, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 19912998 | HCID 19912998 | — |
| Catalyst | Manganese dioxide | HCID 14801 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Product | HCID 19912992 | HCID 19912992 | — |
Reaction Steps
2 g of the thus obtained 2-hydroxymethyl-4-acetylaminopyridine were suspended in 400 ml of dichloromethane, mixed with 6 g of MnO2 and refluxed for 26 hours. The MnO2 was then filtered hot and the dichloromethane solution rotated in to dryness. 1.5 g of 4-acetylaminopyridine-2-aldehyde were obtained.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04997835 |
| Source dataset | uspto-grants-1991_03 |
| ORD ID | ord-5905ec5eaf37463886a8c0c297f7467f |
| Source note | uspto-grants-1991_03 |